Table Of Content

PNNL-22957 EMSP-RPT-018 Prepared for the U.S. Department of Energy under Contract DE-AC05-76RL01830 Investigations into the Nature of Alkaline Soluble, Non-Pertechnetate Technetium BM Rapko TG Levitskaia SA Bryan JM Peterson S Chatterjee RA Peterson MK Edwards SI Sinkov November 2013 ! ! ! ! PNNL-22957 EMSP-RPT-018 Investigations into the Nature of Alkaline Soluble, Non-Pertechnetate Technetium BM Rapko TG Levitskaia SA Bryan JM Peterson S Chatterjee RA Peterson MK Edwards SI Sinkov November 2013 Prepared for the U.S. Department of Energy under Contract DE-AC05-76RL01830 Pacific Northwest National Laboratory Richland, Washington 99352 ! 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PNNL-22957 EMSP-RPT-018 Contents U@'1+*"C'!R+,,-&6!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!"""! =L<(cid:3) D4*&)3+1*")4!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!=(cid:3) =L=(cid:3) d-10A&)+43!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!=(cid:3) =L;(cid:3) GKh'1*"C'%!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!;(cid:3) ;L<(cid:3) P'%+2*%!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!>(cid:3) ;L=(cid:3) #17D:!R64*$'%"%?!F$-&-1*'&".-*")4?!-43!R('1"-*")4!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!>(cid:3) ;L=L=(cid:3) \[+')+%!R64*$'%"%!)5!9&.B#17FG: J!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!>(cid:3) > ;L=L;(cid:3) WW#1BgZP!F$-&-1*'&".-*")4!)5!*$'!\[+')+%!P'-1*")4!Q&)3+1*%!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!`(cid:3) ;L=L>(cid:3) #",'!T'('43'41'!)5!P'-1*")4!Q&)3+1*%!"4!E#17FG: 7GH:7H G: I!R64*$'%'%!LLLLLLLLLLLLLLLLLLLLLLLLLL!](cid:3) > ; ; ;L=Lb(cid:3) #'*&-$63&)5+&-4!R64*$'%"%!)5!9&.B#17FG: J!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!](cid:3) > ;L=L`(cid:3) WW#1!gZP!F$-&-1*'&".-*")4!)5!*$'!#H8!P'-1*")4!Q&)3+1*!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!^(cid:3) ;L=L](cid:3) T"A26,'!R64*$'%"%!)5!9&.B#17FG: J!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!W(cid:3) > ;L=L]L=(cid:3) R64*$'%"%!W!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!=<(cid:3) ;L=L]L;(cid:3) R64*$'%"%!=<!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!==(cid:3) ;L=L]L>(cid:3) R64*$'%"%!==!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!=b(cid:3) ;L;(cid:3) Q&'2","4-&6!R('1"-*")4!\4-26%"%!)5!E#17FG: 7H G: IJ!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!=`(cid:3) > ; > ;L>(cid:3) Q&'(-&-*")4!-43!F$-&-1*'&".-*")4!)5!*$'!E#17FG: 7A2+1)4-*':I;B!F),(2'@!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!;<(cid:3) > ;Lb(cid:3) S2*&-C")2'*!F$-&-1*'&".-*")4!)5!*$'!E#17FG: IJ!R('1"'%!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!;=(cid:3) > ;L`(cid:3) \"&!R*-K"2"*6!)5!*$'!E#17FG: IJ!R('1"'%!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!;;(cid:3) > ;L`L=(cid:3) E#17FG: 7H G: IJ!"4!<L;!Z!HF2!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!;;(cid:3) > ; > ;L`L;(cid:3) E#17FG: 7GH:7H G: I!-*!(H!f!=>L`!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!;b(cid:3) > ; > ;L`L>(cid:3) E#17FG: 7GH:7H G: I!-*!(H!f!^!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!;`(cid:3) > ; ; ;L`Lb(cid:3) E#17FG: 7A2+1)4-*':I;B!"4!<L_!Z!g-GH!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!;](cid:3) > ;L](cid:3) T"%1+%%")4!)5!#17D:!#&"1-&K)462!R64*$'%'%?!R('1"-*")4?!-43!\"&!R*-K"2"*6!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!;_(cid:3) ;L_(cid:3) Z"1&)1-2)&",'*'&!Q'&5)&,-41'!#'%*"4A!+%"4A!F),(2'@-*")4!)5!d-F2 !K6!*$'!! ; Z-1&)1612"1!c"A-43!=^BF&)/4B]!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!><(cid:3) ;L_L=(cid:3) D4*&)3+1*")4!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!><(cid:3) ;L_L;(cid:3) U@('&",'4*-2!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!>;(cid:3) ;L_L;L=(cid:3) D4%*&+,'4*!T'%1&"(*")4!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!>;(cid:3) ;L_L;L;(cid:3) Z"1&)1-2)&",'*&"1!#"*&-*")4!T'*-"2%!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!>>(cid:3) ;L_L;L>(cid:3) P'-A'4*%!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!>>(cid:3) ;L_L;Lb(cid:3) T-*-!Q&)1'%%"4A!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!>>(cid:3) ;L_L>(cid:3) P'%+2*%!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!>b(cid:3) C""! PNNL-22957 EMSP-RPT-018 ;L_Lb(cid:3) T"%1+%%")4!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!b<(cid:3) ;L_L`(cid:3) F)412+%")4%!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!b;(cid:3) ;L^(cid:3) #1!R'4%)&!#-%0!R+,,-&6!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!bb(cid:3) ;L^L=(cid:3) D4*&)3+1*")4!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!bb(cid:3) ;L^L;(cid:3) U@('&",'4*-2!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!bb(cid:3) ;L^L;L=(cid:3) Q&'(-&-*")4!)5!F),(2'@'%!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!b`(cid:3) ;L^L;L=L=(cid:3) P'!F),(2'@'%!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!b`(cid:3) ;L^L;L=L;(cid:3) #1!F),(2'@'%!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!b`(cid:3) ;L^L;L;(cid:3) U2'1*&)1$',"%*&6?!R('1*&)%1)(6?!-43!R('1*&)'2'1*&)1$',"%*&6!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!b`(cid:3) ;L^L;L>(cid:3) R('1*&)'2'1*&)1$',"1-2!R'4%)&!Z'-%+&','4*%!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!b_(cid:3) ;L^L;Lb(cid:3) P'!\4-2)A+'%!)5!#1!R6%*',!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!bW(cid:3) ;L^L>(cid:3) R+,,-&6!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!`>(cid:3) >L<(cid:3) P'5'&'41'%!LLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLLL!``(cid:3) ! ! 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Investigations into the Nature of . species in the aqueous solution even without organic ligands present. Tc in oxidation states lower than VII. 5.

Investigations into the Nature of Alkaline Soluble, Non-Pertechnetate Technetium PDF

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Investigations into the Nature of . species in the aqueous solution even without organic ligands present. Tc in oxidation states lower than VII. 5.

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Publication Year:	2014
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Language:	English
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